Efficient N-formylation of primary aromatic amines using novel solid acid magnetic nanocatalyst

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Clean and Green Approach for N-formylation of Amines using Formic acid under neat reaction condition

In recent years much effort has been carried out on formylations of amines. N-formyl compounds have been widely used in organic synthesis as protecting group of amines [1]. They are also used for synthesis of pharmaceutically important heterocylces [2-5]. Formamides are the Lewis bases, which are known to catalyze reactions such as allylations [6] and hydrosilylations [7] of carbonyl compounds....

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Formylation of amines.

Methods to convert amines to formamides are of interest due to the many uses of formamides as synthetic intermediates. These methods include stoichiometric reactions of formylating reagents and catalytic reactions with CO as the carbonyl source. This review discusses the reported stoichiometric and catalytic approaches for preparation of formamides.

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Preparation of sterically congested 1,3,4-oxadiazole derivatives from N-isocyaniminotriphenylphosphorane, aromatic acids, cyclopentanone and primary amines

Reactions of N-isocyaniminotriphenylphosphorane with cyclopentanone have been studied in the presence of aromatic carboxylic acids and primary amines, proceeds smoothly at room temperature under neutral conditions to afford sterically congested 1,3,4-oxadiazole derivatives by an intramolecular Aza-Wittig cyclization in CH2Cl2 in excellent yields. The structures of the products were deduced from...

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Solid Phase Formylation of N-Terminus Peptides.

Formylation of amino groups is a critical reaction involved in several biological processes including post-translational modification of histones. The addition of a formyl group (CHO) to the N-terminal end of a peptide chain generates biologically active molecules. N-formyl-peptides can be produced by different methods. We performed the N-formylation of two chemotactic hexapetides, Met1-Leu2-Ly...

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ژورنال

عنوان ژورنال: RSC Advances

سال: 2020

ISSN: 2046-2069

DOI: 10.1039/d0ra07476d